Научная статья на тему 'NI-P镀层的制备及其摩擦性能研究'

NI-P镀层的制备及其摩擦性能研究 Текст научной статьи по специальности «Технологии материалов»

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Ключевые слова
表面处理 / 化学镀 / 减摩抗磨 / GCR15 轴承钢

Аннотация научной статьи по технологиям материалов, автор научной работы — 杨晋宇, 肖陟, 胡泽馗, 郑权, 梅顺齐

为提高 GCr15 轴承钢表面性能, 提出一种化学镀工艺, 在 GCr15 轴承钢表面制备 Ni-P 镀层, 利用正交试验方法对 Ni-P 基础镀工艺进行优化, 研究不同的工艺条件下 Ni-P 的显微硬度, 镀速以及微观组织结构, 得出最佳的工艺参数, 并对基体试样和最佳 Ni-P 基础度处理后的试样进行电化学耐腐蚀性能和摩擦磨损性能实验, 检验 Ni-P 镀层对试样的强化效果. 结果表明经化学镀 Ni-P 处理过后, 其化学稳定性和耐磨性都有显著提高.

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RESEARCH ON THE PREPARATION OF NI-P PLATING AND ITS FRICTION PERFORMANCE

In order to improve the surface performance of the GCR15 bearing steel, a chemical plating process is proposed to prepare NI-P plating on the surface of the GCR15 bearing steel, and the orthogonal test method is used to optimize the NI-P basic plating process, and the research conditions are studied. -P's micro-hardness, speed plating, and micro tissue structure, obtain the best process parameters, and perform electrochemical corrosion resistance and friction and wear performance of the substrate sample and the best NI-P basic processing of the basics Experiments, test the reinforcement effect of the Ni-P coating on the sample. Results showed that after the processing of chemical plating NI-P was treated, its chemical stability and abrasion resistance were significantly improved.

Текст научной работы на тему «NI-P镀层的制备及其摩擦性能研究»

For citation-. Yang Jinyu, Xiao Zhi, Hu Zekui, Zheng Quan, Mei Shunqi, Alexey Guryev. Research on the preparation of NI-P plating and its friction performance //

URL. http-//rectors.altstu.ru/ru/periodical/archiv/2022/2/articles/2_8.pdf EDN. https://elibrary.ru/chmwvz

УДК 669

ni-P mmmi&R^Bmmmn

Research on the preparation of NI-P plating

and its friction performance

MW^1, fiffi1, mm1, MM1-2, mm^1, Alexey Guryev1-2

1 «ifg^&smm 430073;

2 rn^rn, e^jj^ 55503s

0

GCr15

mn, mmm&m, ^ifis, mmwMm,

0t, [1-4]. ^

^ffiftK^i^ns [5,5]. Ni-p ^tffflftm ^m&mm^ m, Ni-p iM, 'B^mmx, msm

1 ^rn^m

GCri5 mmn, 1 rn^,

20mmx15mmx5mm X^I^^MS D=1mm ®?L.

01. GCr15 ШММ&0 Table 1.

Composition table of GCr15 bearing steel

C Si Mn Cr Mo Ni P S

0.95-1.05 0.15-0.35 0.25-0.45 1.40-1.65 <0.10 <0.30 <0.025 <0.025

"Ш&ШШЫШ 180#, 320#, 600#, 1000# Ш&ШШШ

Л 80°c ШШШШШШФШШ 5 ШШШ^ШШ 10 ш^шшыт

л 20%hcl тш^шш i

м^^^^шшш&щ^т, m шш, шм, шш&шш.

90°с, титшшлштшш

шы. &ШШШШ 1 тк

ffl 1

1) ^ff; 2) 3)

Fig. 1. Schematic diagram of the experimental setup 1) beaker; 2) magnetic stirrer; 3) sample

2 та&штъ

тш umt-3 шшмш^шодшшшшш, шштяш ШЖШ&, тмжшшмш 2 ш. ъш&шш: 10N, т

^ 2Hz, 5mm, 30mm, 10mm ^ GCr15 Ы

аш^шш. тш sem ттшштшштшяшштш, шшпштштшшгтш, жш^я^шшшшш.

а2шши^ш^й®

Fig. 2. Schematic of friction test system

® 3 (a), (b), (c) ^^ GCr15 ЩШШШ^ШШШШШМШШ, Й® 3 (a)

ш^шшшт шшмдауад, тмштх й^ шшштштй.т, -ш^штм^шшшш«, йшш, штш

ЫЖШВШЩШ. й® 3 (b) яг^ш

шш. а 3 (c) жжшшшмшшт'шшш, ыж-шттш {к^гшттш, шшшшшшшш^. шшшт^шт^т ш, ^^шш^пш^шш^^.

(a) x139 (b) x693 (c) x693

m 3 GCr15 mT^mmwmuwM

Fig. 3. GCr15 bearing steel matrix wear scar morphology

m 4 (a), (b), (c) ffi^ft GCr15 Ni-P ffM^

M 4 (a) "^P, GCr15

Ni-P mmrnmm&^T&^ik,

rnrn&n, «m NI-P mmfornwm&Mwg'X "m^mmrnm. & m 4 (b) ^^m m, ^m&rnMwmmrnm, NI-P fiM^rn^«»^ ^m^mm^rnm, itrnmrn^^mm. ^ ni-P

rnrns^j, sm^mc i^MmiiT»

mj Ni-p 4 (c) m^, m^m^r^m

^WJM, Ni-P fiMM^wn^rn

Ni-P fiM^tt^M^m

(a) x139 (b) x693 (c) x693

m 4 GCr15 «m Ni-p mm^mrnm

Fig. 4. Morphology of wear scars of Ni-P coating on GCr15 bearing steel

3

m 2 ^ 10N 30min mmrnitmrnMR^w^^

GCr15 1302pm, 13.4pm,

mmm^rrn, Ni-p 1023pm, mmm

^ 7.97pm.

M2

Table 2.

Size parameters of wear scars of samples under different strengthening processes

ш ШЙЙЙ (цт) ШММ& (цт)

GCr15 1302 13.4

Ni-p mm 1023 7.97

шшшшш^ш; GCris тшшш Ni-p шт

GCr15 щшм.

¿A® 5 Я&^Ш, GCr15 199.03HV,

Ni-p шмш^ттш^ 634.72HV, шшмтшшт.

а# ní-pos

ffl 5 GCr15 Ni-P

Fig. 5. GCr15 bearing steel Ni-P coating hardness

4 gftm

ft Ni-p GCri5 mmm^mmm&M^kmm,

[1] Mft®. [J]. 2020,30(9):ii9-i28.

[2] ^m^mmmtmM. ní-P úMm [J]. 2020(i): 3i-32.

[3] ?Lí#, ^^Ü, ?LM. A3 Ni-P/Ni-Mo-P [J]. 202i.

[4] Domínguez A.S., Bueno J.J.P., Torres I.Z., et al. Characterization and corrosion resistance of electroless black Ni-P coatings of double black layer on carbon steel [J]. Surface and coatings Technology, 20i7, 326: i92-i99.

[5] Liang X.,Wei K. Research progress of nickel-based electroless plating technologies in protection of metallic materials [J]. Electroplat Finish, 2020,39(i7):ii66-ii70.

[6] Li Y., Liu S., Xue T., et al. Comparison of wear behavior of GCri5 bearing steel prepared by selective laser melting (SLM) and electron beam melting (EBM) [J]. Materials Letters, 202i, 305: i30726.

References

[1] Wang Kun, Hu Feng, Zhou Wen, Wu Kaiming. Current status and development trend of bearing steel research[J]. China Metallurgy,2020,30(9):ii9-i28.

[2]Cui Yigang. Chemical plating of Ni-P alloy coatings on mechanical drive shaft substrates[J]. Electroplating and Environmental Protection, 2020 (i): 3i-32.

[3] Kong Lin, Liu Pinxiao, Kong Bin. Chemical plating of Ni-P/Ni-Mo-P double layer on A3 steel surface[J]. Electroplating and Finishing,202i.

[4] Domínguez A.S., Bueno J.J.P., Torres I.Z., et al. Characterization and corrosion resistance of electroless black Ni-P coatings of double black layer on carbon steel [J]. Surface and coatings Technology, 20i7, 326: i92-i99.

[5] Liang X.,Wei K. Research progress of nickel-based electroless plating technologies in protection of metallic materials [J]. Electroplat Finish, 2020,39(i7):ii66-ii70.

[6] Li Y., Liu S., Xue T., et al. Comparison of wear behavior of GCri5 bearing steel prepared by selective laser melting (SLM) and electron beam melting (EBM) [J]. Materials Letters, 202i, 305: i30726.

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